ECTS credits ECTS credits: 4.5
ECTS Hours Rules/Memories Student's work ECTS: 74.25 Hours of tutorials: 2.25 Expository Class: 18 Interactive Classroom: 18 Total: 112.5
Use languages Spanish, Galician, English
Type: Ordinary Degree Subject RD 1393/2007 - 822/2021
Departments: Inorganic Chemistry, Organic Chemistry
Areas: Inorganic Chemistry, Organic Chemistry
Center Faculty of Chemistry
Call: First Semester
Teaching: With teaching
Enrolment: Enrollable
Once the student has completed Structural Analysis, he or she is expected to be able to
-Knowledge at a practical level the basis of the most important spectroscopic and spectrometric techniques (NMR, EM, UV, IR, etc.) and their potential use for the analysis of chemical structures.
-Predict the most important spectroscopic properties of a chemical substance
-To elucidate molecular structures based on the analysis of their spectroscopic and spectrometric properties.
1- Introduction to structural determination techniques.
2- 1H NMR: fundamentals. Instrumentation. Chemical shift. Spin-spin coupling. Homonuclear and NOE. Practical exercises.
3- 13C NMR: Heteronuclear coupling. Broadband uncoupling. Chemical shifts. DEPT 13C NMR. Introduction to two-dimensional NMR. Practical exercises.
4- Mass spectrometry: Basic principles. Fragmentation mechanisms. Practical exercises.
5- Vibrational spectroscopy: IR and Raman.
6- Application of vibrational spectroscopy to the determination of structures of chemical compounds.
7- Other structural determination techniques.
Basic Bibliography:
- Química Orgánica. K. P. C. Vollhardt y N. E. Schore. Omega. Barcelona, 5ª ed. 2008.
- WADE, L. G. “Química Orgánica”, (5ª edición), Person Education S. A. Madrid, 2004, Capítulos 12 y 13.
- MANFRED HESSE, HERBERT MEIER, BERND ZEEH. "Métodos espectroscópicos en química orgánica" (2ª ed.). Editorial Síntesis, Madrid. 2012.
- E.A.V. EBSWORTH. D.W.H. RANKIN e S. CRADOCK , “Structural methods in Inorganic Chemistry”, Blackwell Scientific Publications, 1987.
Complementary bibliography:
- PRETSCH, E.; BÜHLMANN, P.; AFFOLTER, C.; HERRERA, A.; MARTINEZ, R. "Determinación estructural de compuestos orgánicos". Masson, S.A. Barcelona (2002)
- Problemas a disposición de los alumnos a través del aula virtual.
- JOSÉ RAMÓN PEDRO LLINARES, GONZALO BLAY LLINARES. "200 problemas de determinación estructural de compuestos orgánicos". VISION LIBROS, 2013.
- R. L. CARTER, "Molecular Symmetry ang Group Theory".John Wiley & Sons, , Inc. 1997.
- F.A. COTTON, “La Teoría de grupos aplicada a la Química”, Limusa. 1977
GENERAL COMPETENCIES:
CG2 - Ability to collect and interpreting relevant data, information and results, drawing conclusions and issuing reasoned reports on scientific, technological or other problems requiring the use of knowledge of chemistry.
CG3 - The ability to apply both the theoretical and practical knowledge acquired and the capacity for analysis and abstraction in the definition and presentation of problems and in the search for their solutions in both academic and professional contexts.
CG4 - Ability to communicate, both in writing and orally, knowledge, procedures, results and ideas in Chemistry to a specialised and non-specialised public.
CG5 - Ability of studying and learning autonomously, with the organization of time and resources, new knowledge and techniques in any scientific or technological discipline.
CB1 - That students have demonstrated possession and understanding of knowledge in an area of study that is at the base of general secondary education, and is usually at a level that, although supported by advanced textbooks, also includes some aspects that involve knowledge from the cutting edge of their field of study
SPECIFIC SKILLS:
CE15 - Be able to recognize and analyze new problems and plan strategies to solve them
TRANSVERSAL SKILLS:
TC9 - Develop interpersonal relationship skills.
TC10 - Acquiring critical thinking skills.
TC6 - Performing teamwork.
The evaluation of the competences acquired in the subject will be carried out through the following ways:
In the final exam: CG2, CG3, CG4, CG5, CB1, CE15 and CT10
In tutorial classes: CG5, CT9 and CT6
In seminar classes: CG2, CG3, CG4, CG5, CB1, CE15 CT9, CT10 and CT6.
1. The content of the course will be explained in 14 lectures, including guidelines for the use of the bibliography and for the resolution of problems. These classes will be in the classroom in scenario type 1. In scenario 2 they will be developed through the Virtual Campus (Moodle) or through the Microsoft Teams platform (in the teaching spaces where distance is not possible), or they will be combined up to 50% attendance in those spaces where distance is possible.
In scenario 3 they will be developed in the Microsoft Teams platform and in the digital platform (Moodle).
2. Interactive classes (seminars and tutorials), exercise bulletins and questionnaires will be solved, mainly through the active participation of the students.
The continuous evaluation will be based on the participation in these activities. Usually, problem statements will be available to students in the virtual classroom well in advance. Students should try to solve them autonomously, delivering their solution to the teacher in advance of the seminar classes in which they will be solved. In these classes, the students will present their solutions, which will be analysed by all of them, and the teacher will be in charge of solving the doubts and difficulties that may arise. Occasionally, the seminars will also propose short exercises to be solved on the spot, which will serve to focus on the topics discussed and will be taken into account in the evaluation.
The interactive classes will take place in the classroom during scenario 1
In Scenario 2 it will be possible to combine physical and telematic attendance (Virtual Classroom and Microsoft Teams), up to a maximum of 50% of the hours of the subject in a telematic way, when the distance requires it.
In scenario 3, they will be developed in the Microsoft Teams platform and in the digital platform (Moodle).
Translated with www.DeepL.com/Translator (free version)
3. Group tutorials. Throughout the course, tutorial groups will be organized and used to examine and solve all the doubts in group looking for a greater participation of the student.
These tutorials will be carried out in the classroom during scenario 1, while in scenarios 2 and 3 they will be developed in the Microsoft Teams platform and in the digital platform (Moodle).
4. Personalized tutorials. These are intended to carry out a close monitoring of each student's work.
They will be carried out either in person or virtually, depending on the scenario in which we find ourselves. In any case, in scenarios 2 and 3 they will be "on line" through the Microsoft Teams platform and in the digital platform (Moodle).
5. Digital Platform (Moodle): Through this digital platform a virtual classroom will be kept active in which the teacher will provide the necessary information for the students (PowerPoint files, summaries of topics, problem bulletins and online questionnaires, news, announcements, etc.). It will be the means to use for the final tests in scenario 3.
This platform also contains discussion forums and internal mail which provides excellent communication between teachers and students.
6. Microsoft Teams: The Microsoft Teams group videoconferencing platform will be used to give lectures, depending on the corresponding scenario as indicated above.
The evaluation of this subject will be done through continuous assessment and a final examination. All face-to-face and non face-to-face teaching activities (seminars, tutorials) will be evaluated.
Attendance at interactive classes (seminars and tutorials) is compulsory. Absences must be justified.
It should be noted that the course consists of two different thematic blocks (structural analysis in organic chemistry and structural analysis in inorganic chemistry) and that both will be evaluated according to the criteria specified below. The weight of the qualification of each block will be proportional to the number of hours/credits dedicated to each one of them in the course (57% QO; 43% QI).
The final exam has a weight of 70% in the grade. To pass the course, at least one grade of 4 out of 10 must be obtained in each block (QO and QI) of the final exam. Only in this case will there be an average between the two blocks and continuous assessment.
The continuous evaluation will include the monitoring of the student's personal work by means of written controls, papers submitted and student participation in the classroom, seminars and tutorials. This continuous evaluation will have a percentage weight of 30% in the qualification of the subject and will consist of two components: (a) delivery of exercises solved in the virtual classroom or in class (bulletins, 10%), resolution of exercises in the seminars and tutorials (20%).
Once the cut-off marks of the final exam have been passed, the final grade of each block will be the highest value between two alternatives:
(a) weighted average between the exam and continuous assessment;
(b) exam grade.
The calculation will be made using the following formula:
Final grade = maximum (0.3 x N1 + 0.7 x N2, N2)
N1= numerical score corresponding to continuous assessment (scale 0-10).
N2= numerical score corresponding to the final exam (scale 0-10).
The evaluation of the competences acquired in the subject will be done through the following ways:
In the final exam: CG2, CG3, CG4, CG5, CB1, CE15 and CT10
In tutorial classes: CG5, CT9 and CT6
In seminar classes: CG2, CG3, CG4, CG5, CB1, CE15 CT9, CT10 and CT6.
In scenarios 1 and 2 the final exam will be a classroom exam, while in scenario 3 it will be an online exam through the virtual campus platform (Moodle).
Finally, it should be noted that in the case of fraudulent exercises or tests, the provisions of the "Regulations for the assessment of students' academic performance and the revision of qualifications" will apply.
Hours of attendance:
Lectures: 14 hours
Seminars: 20 hours
Tutorials: 2 hours
Total attendance hours: 36
Non-attendance hours of study of the theoretical part: 25
Non-presential hours of problem solving: 51.5
Total non-attendance hours: 76.5
Evaluation hours: 5
Total workload: 112.5
In order to take advantage of this course successfully, certain previous knowledge of chemistry, seen in previous courses, is necessary. Therefore, it is advisable to have previously studied the following subjects: Physical Chemistry II, Inorganic Chemistry I and II, and Organic Chemistry I and II.
This subject is eminently practical, since it is based on the resolution of problems rather than on the memorization and repetition of contents. Given that these intellectual skills require a period of practice, it is highly advisable that students keep the subject up to date and carry out without delay the exercises that will be proposed in stages.
It is recommended that students use the recommended bibliography. The teachers will advise on the sections of each book that are most appropriate for each topic.
In case of difficulties, students may raise their doubts both in class and in the tutorials.
Contingency Plan (summary).
Class, seminars and tutorials
1. Lectures
Scenario 1, on site.
Scenario 2 synchronous "online" through the Virtual Campus / Microsoft Teams (in teaching spaces where distance is not possible), or may be combined with 50% of face-to-face teaching, in those teaching spaces where it is possible to maintain the distance.
Scenario 3 synchronous "online" through Virtual Campus/Microsoft Teams.
2. Seminars.
Scenario 1 face to face.
Scenario 2 in the classroom or combined with telematic teaching (Virtual Campus/Microsoft Teams) if social distance is not possible.
Scenario 3 synchronous online through Microsoft Teams/Moodle.
3. Tutorials in groups.
Scenario 1 face to face.
Scenario 2 and 3 synchronous "online" through Microsoft Teams/Moodle.
4. Personalized tutoring.
Scenario 1 face to face or online.
Scenarios 2 and 3 synchronous online through Microsoft Teams.
Assessment.
Continuous evaluation (30%).
Bulletins and questionnaires will be handed out through the virtual campus, and the group resolution will be done in the classroom, in scenarios 1 and 2.
While in scenario 3, the delivery of bulletins and questionnaires will be done through the virtual campus, and the group resolution will be done through Microsoft Teams/Moodle.
Final exam (70%).
The final exam will be taken in person in scenarios 1 and 2, while in scenario 3 it will be taken online through the virtual campus platform.
In the case of fraudulent exercises or tests, the provisions of the "Regulations for the assessment of students' academic performance and the revision of qualifications" will apply.
Jose Manuel Vila Abad
- Department
- Inorganic Chemistry
- Area
- Inorganic Chemistry
- Phone
- 881814255
- josemanuel.vila [at] usc.es
- Category
- Professor: University Professor
José Manuel Seco Castro
Coordinador/a- Department
- Organic Chemistry
- Area
- Organic Chemistry
- Phone
- 881814235
- josemanuel.seco [at] usc.es
- Category
- Professor: University Lecturer
Rosa Maria Pedrido Castiñeiras
- Department
- Inorganic Chemistry
- Area
- Inorganic Chemistry
- Phone
- 881814245
- Category
- Professor: University Lecturer
Victor Manuel Sanchez Pedregal
- Department
- Organic Chemistry
- Area
- Organic Chemistry
- Phone
- 881814221
- victor.pedregal [at] usc.es
- Category
- Professor: University Lecturer
| Tuesday | |||
|---|---|---|---|
| 10:00-11:00 | Grupo /CLIS_03 | Spanish | Organic Chemistry Classroom (1st floor) |
| 11:00-12:00 | Grupo /CLE_01 | Spanish | Organic Chemistry Classroom (1st floor) |
| 12:00-13:00 | Grupo /CLIS_02 | Spanish | Organic Chemistry Classroom (1st floor) |
| 13:00-14:00 | Grupo /CLIS_04 | Spanish | Inorganic Chemistry Classroom (1st floor) |
| Wednesday | |||
| 11:00-12:00 | Grupo /CLIS_01 | Spanish | Organic Chemistry Classroom (1st floor) |
| 12:00-13:00 | Grupo /CLE_02 | Spanish | Analytical Chemistry Classroom (2nd floor) |
| Thursday | |||
| 09:00-10:00 | Grupo /CLIS_03 | Spanish | Analytical Chemistry Classroom (2nd floor) |
| 09:00-10:00 | Grupo /CLIS_02 | Spanish | Organic Chemistry Classroom (1st floor) |
| 10:00-11:00 | Grupo /CLIS_01 | Spanish | Organic Chemistry Classroom (1st floor) |
| 12:00-13:00 | Grupo /CLIS_04 | Spanish | Mathematics Classroom (3rd floor) |
| Friday | |||
| 11:00-12:00 | Grupo /CLE_01 | Spanish | Organic Chemistry Classroom (1st floor) |
| 13:00-14:00 | Grupo /CLE_02 | Spanish | Analytical Chemistry Classroom (2nd floor) |
| 01.11.2021 10:00-14:00 | Grupo /CLE_01 | General Chemistry Classroom (2nd floor) |
| 01.11.2021 10:00-14:00 | Grupo /CLE_01 | Inorganic Chemistry Classroom (1st floor) |
| 01.11.2021 10:00-14:00 | Grupo /CLE_01 | Physical Chemistry Classroom (ground floor) |
| 07.01.2021 10:00-14:00 | Grupo /CLE_01 | Mathematics Classroom (3rd floor) |
| 07.01.2021 10:00-14:00 | Grupo /CLE_01 | Physics Classroom (3rd floor) |